In the original languageTranslation into English
STUDY OF THE STRUCTURE OF COMPLEX COMPOUNDS BASED ON 2-AMINO-1,3,4-THIADIZOLE AND ADIPIC ACID OF SALTS OF CO(LL), NI(LL), CU(LL), ZN(LL) USING PHYSICAL MEANS
Authors
Alieva Mushtari Zaylobidin qizi, Nuraliyeva Guzal Abdulhamidovna
Rubric:Chemistry
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Annotation
Complex compounds with heteroligands were synthesized based on 2-amino-1,3,4-thiadiazole, adipic acid and salts of Co(ll), Ni(ll), Cu(ll), Zn(ll). The physicochemical properties of the synthesized complex compounds were studied using IR-spectrum, SEM-EDA and thermal analysis. The results are presented in tables. The chemical structure of complex compounds was determined based on the above results.
Keywords
ligands
metal-complex formers
endothermic and exothermic effects.
IR-spectrum
Coordination compounds
thermal analysis
Authors
Alieva Mushtari Zaylobidin qizi, Nuraliyeva Guzal Abdulhamidovna
Rubric:Chemistry
356
1
Share
356
1
References:
- Atmaram, U.A.; Roopan, S.M. Biological activity of oxadiazole and thiadiazole derivatives // Appl. Microbiol. Biotechnol.- 2022. 106.- P.3489–3505./ [CrossRef] [PubMed]
- Ye Song, Yu-Fei Ji, Min-Yan Kang and Zhi-Liang Liu Acta Crystallographica Section E Structure ReportsISSN 1600-536 Bis(2-amino-5-methyl-1,3,4-thiadiazole-3 )dichloridocobalt(II) // Acta Crystallographica Section E Structure Reports.-2012. doi:10.1107/S1600536812020995
- Masahiko Maekawa, Megumu Munakata, Takayoshi Kuroda-Sowa, Yusaku Suenaga, Kunihisa Sugimoto. Synthesis and crystal structure of tetranuclear copper(I) and silver(I) complexes bridged by 2-amino-1,3,4-thiadiazole(atdz):[Cu4(atdz)6](ClO4)4·2CH3OH and [Ag4(atdz)6](ClO4)4 // 1999. P-153-158.
- Na Wang, Qiu-Yue Lin , Jie Feng, Yu-Ling Zhao, Yan-Jun Wang, Shi-Kun Li Crystal structures, DNA interaction and antiproliferative activities of the cobalt(II) and zinc(II) complexes of 2-amino-1,3,4-thiadiazole with demethylcantharate // Inorganica Chimica Acta № 363.- 2010.- P. 3399–3406.
- Wu Q. et al. Two novel Cu (II) complexes: Synthesis, structure and application in C–H bond activation //Polyhedron. – 2015. – Т. 87. – С. 390-397.
- Nuralieva G.A., Xayrullayev G.U., Kadirova Sh.A. Сhallenges of heterocylical mixed ligand unions with d-metals of acetamid and thiosemikarbazid //Solid state technology63 №6 360-369. 2020.
- Tarasevich B. N. IR spectra of the main classes of organic compounds //Reference materials. – 2012.
- Kazitsyna L. A., Kupletskaya N. B. Application of UV, IR, and NMR spectroscopy in organic chemistry //Vysshaya Shkola, Moscow. – 1971. – С. 23-60.
- Наканиси К. Инфракрасные спектры и строение органических соединений. – Рипол Классик, 2013.
- Уэндландт У. Термические методы анализа // Thermal Methods of Analysis// Пер. с англ. под ред.Степанова В.А. и Берштейна В.А. – М.: Мир, 1978. – C. 526.
- Nuralieva G.A., Aliyeva M. Complex compounds of 2-amino 1,3,4- thiadiazole with 3d-metals and glutar acid // Universum: химия и биология: электрон. научн. журн. 2023. 11(113). URL: https://7universum.com/ru/nature/archive/item/16087
- Marshall J. L. Scanning electron microscopy and energy dispersive X-ray (SEM/EDX) characterization of solder solderability and reliability //Solder joint reliability: theory and applications. – Boston, MA: Springer US, 1991. – С. 173-224.
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